Crystallography Open Database

Information card for entry 4115966

Preview

Coordinates	4115966.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H36 N Si3 Y
Calculated formula	C26 H36 N Si3 Y
Title of publication	C2-Symmetric ansa-Lanthanidocene Complexes. Synthesis via Silylamine Elimination and β-SiH Agostic Rigidity
Authors of publication	Jörg Eppinger; Michael Spiegler; Wolfgang Hieringer; Wolfgang A. Herrmann; Reiner Anwander
Journal of publication	Journal of the American Chemical Society
Year of publication	2000
Journal volume	122
Pages of publication	3080 - 3096
a	15.11 ± 0.004 Å
b	11.731 ± 0.002 Å
c	15.699 ± 0.005 Å
α	90°
β	108.55 ± 0.01°
γ	90°
Cell volume	2638.2 ± 1.2 Å³
Cell temperature	163 K
Ambient diffraction temperature	163 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0318
Residual factor for significantly intense reflections	0.0318
Weighted residual factors for all reflections	0.0742
Weighted residual factors for significantly intense reflections	0.0742
Goodness-of-fit parameter for all reflections	1.048
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4115966.html