Crystallography Open Database

Information card for entry 4115968

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Coordinates	4115968.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C75 H88 N2 Si6 Y2
Calculated formula	C75 H88 N2 Si6 Y2
Title of publication	C2-Symmetric ansa-Lanthanidocene Complexes. Synthesis via Silylamine Elimination and β-SiH Agostic Rigidity
Authors of publication	Jörg Eppinger; Michael Spiegler; Wolfgang Hieringer; Wolfgang A. Herrmann; Reiner Anwander
Journal of publication	Journal of the American Chemical Society
Year of publication	2000
Journal volume	122
Pages of publication	3080 - 3096
a	11.1193 ± 0.0006 Å
b	11.9449 ± 0.0005 Å
c	14.8399 ± 0.0008 Å
α	72.396 ± 0.005°
β	75.824 ± 0.006°
γ	69.896 ± 0.005°
Cell volume	1742.24 ± 0.17 Å³
Cell temperature	193 K
Ambient diffraction temperature	193 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0358
Residual factor for significantly intense reflections	0.0358
Weighted residual factors for all reflections	0.0944
Weighted residual factors for significantly intense reflections	0.0944
Goodness-of-fit parameter for all reflections	0.973
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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