Information card for entry 4115987

Structure parameters

• Chemical name: Tris(tetrahydofuran)(iodo)(2,6-(diphenyl)phenyl)ytterbium(II) hemi tetrahydrofuran solvate
• Formula: C32 H41 I O3.5 Yb
• Calculated formula: C32 H41 I O3.5 Yb
• Title of publication: Synthesis and First Structural Characterization of Lanthanide(II) Aryls: Observation of a Schlenk Equilibrium in Europium(II) and Ytterbium(II) Chemistry
• Authors of publication: Gernot Heckmann; Mark Niemeyer
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2000
• Journal volume: 122
• Pages of publication: 4227 - 4228
• a: 7.887 ± 0.001 Å
• b: 11.114 ± 0.002 Å
• c: 35.472 ± 0.005 Å
• α: 90°
• β: 94.68 ± 0.01°
• γ: 90°
• Cell volume: 3099 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.056
• Residual factor for significantly intense reflections: 0.0378
• Weighted residual factors for significantly intense reflections: 0.0842
• Weighted residual factors for all reflections included in the refinement: 0.0917
• Goodness-of-fit parameter for all reflections included in the refinement: 1.243
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No