Crystallography Open Database

Information card for entry 4116212

Preview

Coordinates	4116212.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C10 H32 Mo10 O33 Rb4 S10
Calculated formula	C10 Mo10 O33 Rb4 S10
Title of publication	"Wheeling Templates" in Molecular Oxothiomolybdate Rings: Syntheses, Structures, and Dynamics
Authors of publication	Bernadette Salignac; Sandra Riedel; Anne Dolbecq; Francis Sécheresse; Emmanuel Cadot
Journal of publication	Journal of the American Chemical Society
Year of publication	2000
Journal volume	122
Pages of publication	10381 - 10389
a	24.296 ± 0.004 Å
b	10.165 ± 0.003 Å
c	21.828 ± 0.006 Å
α	90°
β	90°
γ	90°
Cell volume	5391 ± 2 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	6
Space group number	36
Hermann-Mauguin space group symbol	C m c 21
Hall space group symbol	C 2c -2
Residual factor for all reflections	0.1167
Residual factor for significantly intense reflections	0.06
Weighted residual factors for all reflections	0.1593
Weighted residual factors for significantly intense reflections	0.1294
Goodness-of-fit parameter for all reflections	1.114
Goodness-of-fit parameter for significantly intense reflections	1.125
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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