Crystallography Open Database

Information card for entry 4116260

Preview

Coordinates	4116260.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H45 F U
Calculated formula	C30 H45 F2 U
Title of publication	How Much Steric Crowding Is Possible in Tris(η5-pentamethylcyclopentadienyl) Complexes? Synthesis and Structure of (C5Me5)3UCl and (C5Me5)3UF1
Authors of publication	William J. Evans; Gregory W. Nyce; Matthew A. Johnston; Joseph W. Ziller
Journal of publication	Journal of the American Chemical Society
Year of publication	2000
Journal volume	122
Pages of publication	12019 - 12020
a	9.9804 ± 0.0005 Å
b	9.9804 ± 0.0005 Å
c	15.4529 ± 0.0011 Å
α	90°
β	90°
γ	120°
Cell volume	1333.02 ± 0.13 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	4
Space group number	176
Hermann-Mauguin space group symbol	P 63/m
Hall space group symbol	-P 6c
Residual factor for all reflections	0.0609
Residual factor for significantly intense reflections	0.0434
Weighted residual factors for significantly intense reflections	0.108
Weighted residual factors for all reflections included in the refinement	0.127
Goodness-of-fit parameter for all reflections included in the refinement	1.18
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4116260.html