Information card for entry 4116288

Structure parameters

• Common name: [Cp*RuCl(SPh)]2
• Formula: C32 H40 Cl2 Ru2 S2
• Calculated formula: C64 H80 Cl4 Ru4 S4
• Title of publication: First Transition-Metal Complex Catalyzed Addition of Organic Disulfides to Alkenes Enables the Rapid Synthesis of vicinal-Dithioethers
• Authors of publication: Teruyuki Kondo; Shin-ya Uenoyama; Ken-ichi Fujita; Take-aki Mitsudo
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 1999
• Journal volume: 121
• Pages of publication: 482 - 483
• a: 11.873 ± 0.004 Å
• b: 9.556 ± 0.004 Å
• c: 14.089 ± 0.003 Å
• α: 90°
• β: 92.13 ± 0.02°
• γ: 90°
• Cell volume: 1597.4 ± 0.9 ų
• Cell temperature: 296.2 K
• Ambient diffraction temperature: 296.2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0428
• Residual factor for significantly intense reflections: 0.0428
• Weighted residual factors for significantly intense reflections: 0.0459
• Weighted residual factors for all reflections included in the refinement: 0.0459
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No