Information card for entry 4116319

Structure parameters

• Formula: C24 H34 N4 Ni O
• Calculated formula: C26 H34 N4 Ni O0.5
• Title of publication: Reactions of Transition-Metal Metallocenes with Stable Carbenes
• Authors of publication: Colin D. Abernethy; Jason A. C. Clyburne; Alan H. Cowley; Richard A. Jones
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 1999
• Journal volume: 121
• Pages of publication: 2329 - 2330
• a: 11.165 ± 0.003 Å
• b: 9.693 ± 0.002 Å
• c: 23.201 ± 0.005 Å
• α: 90°
• β: 95.82 ± 0.02°
• γ: 90°
• Cell volume: 2497.9 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0847
• Residual factor for significantly intense reflections: 0.055
• Weighted residual factors for all reflections: 0.2675
• Weighted residual factors for significantly intense reflections: 0.1736
• Goodness-of-fit parameter for all reflections: 1.03
• Goodness-of-fit parameter for significantly intense reflections: 0.843
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No