Information card for entry 4116360

Structure parameters

• Formula: C17 H24 O2 Si2
• Calculated formula: C17 H24 O2 Si2
• SMILES: [Si](C1=C([Si](C)(C)C)/C(=C/c2ccccc2)OC1=O)(C)(C)C
• Title of publication: Reactions of the "Stable" Nitroxyl Radical TEMPO with Ketenes: Formation of a Unique Peroxidic Source of Aminyl Radicals
• Authors of publication: Wen-wei Huang; Huda Henry-Riyad; Thomas T. Tidwell
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 1999
• Journal volume: 121
• Pages of publication: 3939 - 3943
• a: 9.3238 ± 0.0004 Å
• b: 11.4506 ± 0.0004 Å
• c: 34.2187 ± 0.0013 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3653.3 ± 0.2 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0669
• Residual factor for significantly intense reflections: 0.0434
• Weighted residual factors for significantly intense reflections: 0.1078
• Weighted residual factors for all reflections included in the refinement: 0.117
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No