Crystallography Open Database

Information card for entry 4116389

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Coordinates	4116389.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C180 H180 Fe4 Mo8 N16 O32
Calculated formula	C179.68 H152 Fe4 Mo8 N16 O32
Title of publication	Square and Triangular Arrays Based on Mo24+ and Rh24+ Units
Authors of publication	F. Albert Cotton; Lee M. Daniels; Chun Lin; Carlos A. Murillo
Journal of publication	Journal of the American Chemical Society
Year of publication	1999
Journal volume	121
Pages of publication	4538 - 4539
a	16.951 ± 0.003 Å
b	17.07 ± 0.01 Å
c	20.935 ± 0.008 Å
α	103.84 ± 0.02°
β	104.85 ± 0.04°
γ	105.92 ± 0.03°
Cell volume	5309 ± 4 Å³
Cell temperature	273 ± 2 K
Ambient diffraction temperature	273 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1225
Residual factor for significantly intense reflections	0.0846
Weighted residual factors for all reflections	0.2508
Weighted residual factors for significantly intense reflections	0.2056
Goodness-of-fit parameter for all reflections	1.077
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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