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Information card for entry 4116443
Preview
Coordinates | 4116443.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C42 H50 I2 P2 Ru S |
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Calculated formula | C42 H50 P2 Ru Si2 |
SMILES | [RuH3]1([P](c2ccccc2)(c2ccccc2)c2ccccc2)([P](c2ccccc2)(c2ccccc2)c2ccccc2)[H][Si](CC[Si]1(C)C)(C)C |
Title of publication | Ruthenium Complexes Containing Two Ru-(η2-Si-H) Bonds: Synthesis, Spectroscopic Properties, Structural Data, Theoretical Calculations, and Reactivity Studies |
Authors of publication | Fabien Delpech; Sylviane Sabo-Etienne; Jean-Claude Daran; Bruno Chaudret; Khansaa Hussein; Colin J. Marsden; Jean-Claude Barthelat |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 1999 |
Journal volume | 121 |
Journal issue | 28 |
Pages of publication | 6668 - 6682 |
a | 18.072 ± 0.003 Å |
b | 10.7807 ± 0.0011 Å |
c | 20.773 ± 0.003 Å |
α | 90° |
β | 106.855 ± 0.018° |
γ | 90° |
Cell volume | 3873.3 ± 1 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for significantly intense reflections | 0.0268 |
Weighted residual factors for significantly intense reflections | 0.0278 |
Goodness-of-fit parameter for significantly intense reflections | 1.0645 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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