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Information card for entry 4116571
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Coordinates | 4116571.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | g-lactam 4 |
---|---|
Chemical name | 3S-Hydroxy-2R-(1S-hydroxy-2-methyl-propyl)-4R-n-propyl-5- oxo-pyrrolidine-2-carboxylic acid methyl ester |
Formula | C13 H23 N O5 |
Calculated formula | C13 H23 N O5 |
SMILES | O=C1N[C@@]([C@@H](O)[C@H]1CCC)([C@@H](O)C(C)C)C(=O)OC |
Title of publication | A Novel and Efficient Synthesis of a Highly Active Analogue of clasto-Lactacystin β-Lactone |
Authors of publication | François Soucy; Louis Grenier; Mark L. Behnke; Antonia T. Destree; Teresa A. McCormack; Julian Adams; Louis Plamondon |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 1999 |
Journal volume | 121 |
Pages of publication | 9967 - 9976 |
a | 10.536 ± 0.002 Å |
b | 20.451 ± 0.004 Å |
c | 27.557 ± 0.006 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 5938 ± 2 Å3 |
Cell temperature | 213 ± 2 K |
Ambient diffraction temperature | 213 ± 2 K |
Number of distinct elements | 4 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.1156 |
Residual factor for significantly intense reflections | 0.0736 |
Weighted residual factors for significantly intense reflections | 0.1714 |
Weighted residual factors for all reflections included in the refinement | 0.1957 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.026 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4116571.html
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Users of the data should acknowledge the original authors of the
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