Information card for entry 4116633

Structure parameters

• Formula: C14 H36 B2 F8 Ni P4
• Calculated formula: C14 H36 B2 F8 Ni P4
• Title of publication: Relative Hydride, Proton, and Hydrogen Atom Transfer Abilities of [HM(diphosphine)2]PF6 Complexes (M = Pt, Ni)
• Authors of publication: Douglas E. Berning; Bruce C. Noll; Daniel L. DuBois
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 1999
• Journal volume: 121
• Pages of publication: 11432 - 11447
• a: 9.8371 ± 0.0013 Å
• b: 16.764 ± 0.003 Å
• c: 14.8801 ± 0.0018 Å
• α: 90°
• β: 101.136 ± 0.007°
• γ: 90°
• Cell volume: 2407.7 ± 0.6 ų
• Cell temperature: 160 ± 2 K
• Ambient diffraction temperature: 160 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0354
• Residual factor for significantly intense reflections: 0.0286
• Weighted residual factors for significantly intense reflections: 0.0672
• Weighted residual factors for all reflections included in the refinement: 0.0716
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No