Information card for entry 4116706

Structure parameters

• Formula: C15 H33 N Nb O3 P3 Si
• Calculated formula: C14 H32.5 N0.5 Nb0.5 O2.5 P2.5 Si0.5
• Title of publication: The First Nitrosyl Complexes of Niobium and Tantalum
• Authors of publication: P. James Daff; Peter Legzdins; Steven J. Rettig
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 1998
• Journal volume: 120
• Pages of publication: 2688 - 2689
• a: 16.5158 ± 0.001 Å
• b: 13.6408 ± 0.0008 Å
• c: 10.426 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2348.9 ± 0.5 ų
• Cell temperature: 180.2 K
• Ambient diffraction temperature: 180.2 K
• Number of distinct elements: 7
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.098
• Weighted residual factors for all reflections: 0.0717
• Goodness-of-fit parameter for all reflections: 2.225
• Goodness-of-fit parameter for all reflections included in the refinement: 2.22
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No