Information card for entry 4116710

Structure parameters

• Formula: C24 H32 Cl F6 N Ni P4
• Calculated formula: C24 H32 Cl F5.98 N Ni P4
• Title of publication: Synthesis and Characterization of the First Mononuclear NiII Phosphorane Imino Complex
• Authors of publication: Laura Crociani; Francesco Tisato; Fiorenzo Refosco; Giuliano Bandoli; Benedetto Corain; Luigi M. Venanzi
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 1998
• Journal volume: 120
• Pages of publication: 2973 - 2974
• a: 14.464 ± 0.004 Å
• b: 12.007 ± 0.004 Å
• c: 18.518 ± 0.005 Å
• α: 90°
• β: 110.17 ± 0.02°
• γ: 90°
• Cell volume: 3018.8 ± 1.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.108
• Residual factor for significantly intense reflections: 0.0627
• Weighted residual factors for all reflections: 0.2022
• Weighted residual factors for significantly intense reflections: 0.1699
• Goodness-of-fit parameter for all reflections: 1.16
• Goodness-of-fit parameter for significantly intense reflections: 1.19
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No