Information card for entry 4116841

Structure parameters

• Formula: C2 Cs6 O44 Rh Si W11
• Calculated formula: C2 Cs6 O44 Rh Si W11
• Title of publication: Rhodium-Carbon Bond Formation in Aqueous Solution. Synthesis, Structure, and Reactivity of the Functionalized Heteropolytungstates, [XW11O39RhCH2COOH]5,6- (X = P, Si)
• Authors of publication: Xinyi Wei; Michael H. Dickman; Michael T. Pope
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 1998
• Journal volume: 120
• Pages of publication: 10254 - 10255
• a: 11.2577 ± 0.0002 Å
• b: 22.9293 ± 0.0005 Å
• c: 17.6274 ± 0.0004 Å
• α: 90°
• β: 94.408 ± 0.001°
• γ: 90°
• Cell volume: 4536.72 ± 0.16 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.082
• Residual factor for significantly intense reflections: 0.0667
• Weighted residual factors for all reflections: 0.1708
• Weighted residual factors for significantly intense reflections: 0.1612
• Goodness-of-fit parameter for all reflections: 1.113
• Goodness-of-fit parameter for significantly intense reflections: 1.159
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No