Crystallography Open Database

Information card for entry 4116970

Preview

Coordinates	4116970.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C69 H54 Cl2 Cr2 N4 O4 P4
Calculated formula	C272 Cr8 N16 O16 P16
Title of publication	Elongation of the Quadruple CrII-CrII Bond Induced by Two PtMe2 Moieties in the Linearly Aligned Tetrametal System, PtMe2...Cr-Cr...PtMe2
Authors of publication	Kazushi Mashima; Mitsuhiro Tanaka; Kazuhide Tani; Akira Nakamura; Sadamu Takeda; Wasuke Mori; Kizashi Yamaguchi
Journal of publication	Journal of the American Chemical Society
Year of publication	1997
Journal volume	119
Pages of publication	4307 - 4308
a	18.645 ± 0.005 Å
b	17.896 ± 0.003 Å
c	19.338 ± 0.003 Å
α	90°
β	104.12 ± 0.02°
γ	90°
Cell volume	6258 ± 2 Å³
Cell temperature	23 K
Ambient diffraction temperature	23 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/a 1
Hall space group symbol	-P 2yab
Residual factor for significantly intense reflections	0.072
Weighted residual factors for significantly intense reflections	0.069
Goodness-of-fit parameter for significantly intense reflections	2.01
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKalpha
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4116970.html