Information card for entry 4116972

Structure parameters

• Formula: C19 H31 I O3 Si
• Calculated formula: C19 H31 I O3 Si
• Title of publication: Total Synthesis of (-)-Dendrobine via α-Carbonyl Radical Cyclization
• Authors of publication: Chin-Kang Sha; Rei-Torng Chiu; Cheng-Fen Yang; Nai-Tung Yao; Wei-Hong Tseng; Fen-Ling Liao; Sue-Lein Wang
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 1997
• Journal volume: 119
• Pages of publication: 4130 - 4135
• a: 16.377 ± 0.002 Å
• b: 29.029 ± 0.002 Å
• c: 8.932 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4246.3 ± 1.1 ų
• Cell temperature: 297 K
• Number of distinct elements: 5
• Space group number: 18
• Hermann-Mauguin space group symbol: P 21 21 2
• Hall space group symbol: P 2 2ab
• Residual factor for significantly intense reflections: 0.0448
• Weighted residual factors for significantly intense reflections: 0.0543
• Goodness-of-fit parameter for significantly intense reflections: 0.88
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No