Crystallography Open Database

Information card for entry 4117090

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Coordinates	4117090.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C76 H71 O4 P2 Rh
Calculated formula	C76 H71 O4 P2 Rh
Title of publication	π-Allylic Rhodium Complex Catalyzed Living Copolymerization of Arylallenes with Carbon Monoxide To Give Structurally Regulated Polyketones
Authors of publication	Kohtaro Osakada; Jun-chul Choi; Takakazu Yamamoto
Journal of publication	Journal of the American Chemical Society
Year of publication	1997
Journal volume	119
Pages of publication	12390 - 12391
a	14.132 ± 0.003 Å
b	18.519 ± 0.007 Å
c	12.177 ± 0.005 Å
α	102.13 ± 0.03°
β	95.35 ± 0.03°
γ	95.6 ± 0.02°
Cell volume	3079.6 ± 1.9 Å³
Cell temperature	23 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.062
Weighted residual factors for all reflections included in the refinement	0.044
Goodness-of-fit parameter for all reflections included in the refinement	3.23
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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