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Information card for entry 4117149
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Coordinates | 4117149.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C63 H60 Au4 Cl8 Fe O8 P4 S |
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Calculated formula | C63 H54 Au4 Cl8.02 Fe O8 P4 S |
Title of publication | Aurophilicity at Sulfur Centers. Synthesis and Reactivity of the Complex [S(Au2dppf)]; Formation of Polynuclear Sulfur-Centered Complexes. Crystal Structures of [S(Au2dppf)].2CHCl3, [(μ-Au2dppf){S(Au2dppf)}2](OTf)2. 8CHCl3, and [S(AuPPh2Me)2(Au2dppf)](ClO4)2.3CH2Cl2 |
Authors of publication | Fernando Canales; M. Concepción Gimeno; Antonio Laguna; Peter G. Jones |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 1996 |
Journal volume | 118 |
Pages of publication | 4839 - 4845 |
a | 13.727 ± 0.002 Å |
b | 15.952 ± 0.003 Å |
c | 17.763 ± 0.002 Å |
α | 71.738 ± 0.012° |
β | 73.264 ± 0.014° |
γ | 75.96 ± 0.02° |
Cell volume | 3487.3 ± 1 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1371 |
Residual factor for significantly intense reflections | 0.0768 |
Weighted residual factors for all reflections | 0.1945 |
Weighted residual factors for significantly intense reflections | 0.157 |
Goodness-of-fit parameter for all reflections | 1.086 |
Goodness-of-fit parameter for significantly intense reflections | 1.117 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4117149.html
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