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Information card for entry 4117154
Preview
Coordinates | 4117154.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C13 H36 Al2 Cl5 N3 Si3 |
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Calculated formula | C13 H36 Al2 Cl5 N3 Si3 |
SMILES | [Al]12(Cl)[NH](CC[N]1(CCN2[Si](C)(C)C)[Si](C)(C)C)[Si](C)(C)C.[Al](Cl)(Cl)(Cl)[Cl-] |
Title of publication | Synthesis and Structure of the First Chiral Tetracoordinated Aluminum Cation |
Authors of publication | Norbert Emig; Régis Réau; Harald Krautscheid; Dieter Fenske; Guy Bertrand |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 1996 |
Journal volume | 118 |
Pages of publication | 5822 - 5823 |
a | 9.992 ± 0.004 Å |
b | 11.97 ± 0.004 Å |
c | 13.16 ± 0.005 Å |
α | 82.62 ± 0.03° |
β | 68.94 ± 0.03° |
γ | 89.17 ± 0.03° |
Cell volume | 1455.8 ± 1 Å3 |
Cell temperature | 200 ± 2 K |
Ambient diffraction temperature | 200 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0559 |
Residual factor for significantly intense reflections | 0.0374 |
Weighted residual factors for all reflections | 0.1026 |
Weighted residual factors for significantly intense reflections | 0.0916 |
Goodness-of-fit parameter for all reflections | 1.034 |
Goodness-of-fit parameter for significantly intense reflections | 1.06 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKa |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4117154.html
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