Crystallography Open Database

Information card for entry 4117165

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Coordinates	4117165.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C74 H64 Cl16 Mo2 N4 O4 P4 Pd2
Calculated formula	C304 H240 Cl80 Mo8 N16 O16 P16 Pd8
Title of publication	Reductive Formation of Straight Linear Metal-Metal Bonded Tetranuclear Complexes X-M-Mo-Mo-M-X from X2M...Mo-Mo...MX2 Supported by Four Tridentate 6-Diphenylphosphino-2-pyridonate Ligands (M = Pd, Pt; X = Cl, Br, I)
Authors of publication	Kazushi Mashima; Hiroshi Nakano; Akira Nakamura
Journal of publication	Journal of the American Chemical Society
Year of publication	1996
Journal volume	118
Pages of publication	9083 - 9095
a	24.262 ± 0.004 Å
b	12.3 ± 0.003 Å
c	31.521 ± 0.006 Å
α	90°
β	112.86 ± 0.01°
γ	90°
Cell volume	8668 ± 3 Å³
Cell temperature	23 K
Ambient diffraction temperature	23 K
Number of distinct elements	8
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for significantly intense reflections	0.084
Weighted residual factors for significantly intense reflections	0.064
Goodness-of-fit parameter for significantly intense reflections	2.97
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKalpha
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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