Information card for entry 4117171

Structure parameters

• Formula: C69 H54 Br2 Cl2 Mo2 N4 O4 P4 Pt2
• Calculated formula: C276 H216 Br8 Cl8 Mo8 N16 O16 P16 Pt8
• Title of publication: Reductive Formation of Straight Linear Metal-Metal Bonded Tetranuclear Complexes X-M-Mo-Mo-M-X from X2M...Mo-Mo...MX2 Supported by Four Tridentate 6-Diphenylphosphino-2-pyridonate Ligands (M = Pd, Pt; X = Cl, Br, I)
• Authors of publication: Kazushi Mashima; Hiroshi Nakano; Akira Nakamura
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 1996
• Journal volume: 118
• Pages of publication: 9083 - 9095
• a: 16.077 ± 0.003 Å
• b: 16.592 ± 0.003 Å
• c: 27.861 ± 0.002 Å
• α: 90°
• β: 96.106 ± 0.01°
• γ: 90°
• Cell volume: 7390 ± 2 ų
• Cell temperature: 23 K
• Ambient diffraction temperature: 23 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.053
• Weighted residual factors for significantly intense reflections: 0.069
• Goodness-of-fit parameter for significantly intense reflections: 1.82
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No