Crystallography Open Database

Information card for entry 4117179

Preview

Coordinates	4117179.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H24 Co2 O7
Calculated formula	C22 H24 Co2 O7
Title of publication	Intermediate Complexes in the Octacarbonyl Dicobalt-Initiated Living Polymerization of 3-Methyl-1,2-butadiene
Authors of publication	Judit Sóvágó; M. Gary Newton; Evgenia A. Mushina; Ferenc Ungváry
Journal of publication	Journal of the American Chemical Society
Year of publication	1996
Journal volume	118
Pages of publication	9589 - 9596
a	17.732 ± 0.001 Å
b	7.0943 ± 0.0007 Å
c	20.284 ± 0.003 Å
α	90°
β	109.246 ± 0.008°
γ	90°
Cell volume	2409 ± 0.5 Å³
Cell temperature	296.2 K
Ambient diffraction temperature	296.2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/a 1
Hall space group symbol	-P 2yab
Residual factor for significantly intense reflections	0.0447
Weighted residual factors for significantly intense reflections	0.0448
Goodness-of-fit parameter for significantly intense reflections	2.827
Diffraction radiation wavelength	1.5418 Å
Diffraction radiation type	CuKalpha
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4117179.html