Crystallography Open Database

Information card for entry 4117292

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Coordinates	4117292.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H39 N O U
Calculated formula	C27 H39 N O U
Title of publication	Synthesis, Structure, and Magnetism of an f Element Nitrosyl Complex, (C5Me4H)3UNO
Authors of publication	Nathan A. Siladke; Katie R. Meihaus; Joseph W. Ziller; Ming Fang; Filipp Furche; Jeffrey R. Long; William J. Evans
Journal of publication	Journal of the American Chemical Society
Year of publication	2012
Journal volume	134
Pages of publication	1243 - 1249
a	13.4239 ± 0.0007 Å
b	13.4239 ± 0.0007 Å
c	13.4239 ± 0.0007 Å
α	90°
β	90°
γ	90°
Cell volume	2419 ± 0.2 Å³
Cell temperature	93 ± 2 K
Ambient diffraction temperature	93 ± 2 K
Number of distinct elements	5
Space group number	198
Hermann-Mauguin space group symbol	P 21 3
Hall space group symbol	P 2ac 2ab 3
Residual factor for all reflections	0.0164
Residual factor for significantly intense reflections	0.0158
Weighted residual factors for significantly intense reflections	0.0339
Weighted residual factors for all reflections included in the refinement	0.0342
Goodness-of-fit parameter for all reflections included in the refinement	1.098
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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