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Information card for entry 4117333
Preview
Coordinates | 4117333.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | As4 H214 Li10 Mo12 O246 Rb14 S12 W36 |
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Calculated formula | As4 Mo12 O183.4 Rb9.9 S12 W36 |
Title of publication | Polyoxometalates Paneling through {Mo~2~O~2~S~2~} Coordination: Cation-Directed Conformations and Chemistry of a Supramolecular Hexameric Scaffold |
Authors of publication | Jérôme Marrot; Marie Anne Pilette; Mohamed Haouas; Sébastien Floquet; Francis Taulelle; Xavier López; Josep M. Poblet; Emmanuel Cadot |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2012 |
Journal volume | 134 |
Pages of publication | 1724 - 1737 |
a | 47.4379 ± 0.001 Å |
b | 18.6347 ± 0.0003 Å |
c | 36.2086 ± 0.0007 Å |
α | 90° |
β | 127.567 ± 0.001° |
γ | 90° |
Cell volume | 25370.9 ± 0.9 Å3 |
Cell temperature | 296 ± 2 K |
Ambient diffraction temperature | 296 ± 2 K |
Number of distinct elements | 8 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.1008 |
Residual factor for significantly intense reflections | 0.0588 |
Weighted residual factors for significantly intense reflections | 0.1731 |
Weighted residual factors for all reflections included in the refinement | 0.2178 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.062 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4117333.html
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