Information card for entry 4117765

Structure parameters

• Formula: C31.5 H32 U
• Calculated formula: C31.5 H32 U
• Title of publication: Carbon-Carbon Reductive Elimination from Homoleptic Uranium(IV) Alkyls Induced by Redox-Active Ligands
• Authors of publication: Steven J. Kraft; Phillip E. Fanwick; Suzanne C. Bart
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2012
• Journal volume: 134
• Pages of publication: 6160 - 6168
• a: 14.7003 ± 0.0006 Å
• b: 9.6373 ± 0.0005 Å
• c: 17.7689 ± 0.0007 Å
• α: 90°
• β: 96.316 ± 0.003°
• γ: 90°
• Cell volume: 2502.06 ± 0.19 ų
• Cell temperature: 150 ± 0.2 K
• Ambient diffraction temperature: 150 ± 0.2 K
• Number of distinct elements: 3
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.047
• Residual factor for significantly intense reflections: 0.046
• Weighted residual factors for significantly intense reflections: 0.132
• Weighted residual factors for all reflections included in the refinement: 0.134
• Goodness-of-fit parameter for all reflections included in the refinement: 1.134
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CU-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No