Information card for entry 4117831

Structure parameters

• Chemical name: Si{B(NDippCH)2}{N(Dipp)SiMe3}
• Formula: C52 H72 B2 N4 Sn
• Calculated formula: C52 H72 B2 N4 Sn
• Title of publication: A Stable Two-Coordinate Acyclic Silylene
• Authors of publication: Andrey V. Protchenko; Krishna Hassomal Birjkumar; Deepak Dange; Andrew D. Schwarz; Dragoslav Vidovic; Cameron Jones; Nikolas Kaltsoyannis; Philip Mountford; Simon Aldridge
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2012
• Journal volume: 134
• Pages of publication: 6500 - 6503
• a: 12.7468 ± 0.0003 Å
• b: 20.3216 ± 0.0005 Å
• c: 19.4027 ± 0.0005 Å
• α: 90°
• β: 94.8071 ± 0.0011°
• γ: 90°
• Cell volume: 5008.3 ± 0.2 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1288
• Residual factor for significantly intense reflections: 0.1026
• Weighted residual factors for all reflections: 0.2675
• Weighted residual factors for significantly intense reflections: 0.246
• Weighted residual factors for all reflections included in the refinement: 0.2675
• Goodness-of-fit parameter for all reflections included in the refinement: 0.957
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No