Information card for entry 4117833

Structure parameters

• Chemical name: Ge{B(NDippCH)2}{N(SiMe3)Dipp*}
• Formula: C64.5 H78 B Ge N3 Si
• Calculated formula: C64.5 H78 B Ge N3 Si
• Title of publication: A Stable Two-Coordinate Acyclic Silylene
• Authors of publication: Andrey V. Protchenko; Krishna Hassomal Birjkumar; Deepak Dange; Andrew D. Schwarz; Dragoslav Vidovic; Cameron Jones; Nikolas Kaltsoyannis; Philip Mountford; Simon Aldridge
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2012
• Journal volume: 134
• Pages of publication: 6500 - 6503
• a: 12.3688 ± 0.0005 Å
• b: 12.5625 ± 0.0005 Å
• c: 19.8714 ± 0.0007 Å
• α: 99.87 ± 0.003°
• β: 103.835 ± 0.003°
• γ: 100.901 ± 0.003°
• Cell volume: 2867 ± 0.2 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0574
• Residual factor for significantly intense reflections: 0.0415
• Weighted residual factors for significantly intense reflections: 0.0887
• Weighted residual factors for all reflections included in the refinement: 0.0957
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No