Information card for entry 4118198

Structure parameters

• Formula: C48 H96 O10 Rh2
• Calculated formula: C48 H96 O10 Rh2
• Title of publication: Rh-Catalyzed Intermolecular Reactions of Cyclic α-Diazocarbonyl Compounds with Selectivity over Tertiary C-H Bond Migration
• Authors of publication: Andrew DeAngelis; Olga Dmitrenko; Joseph M. Fox
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2012
• Journal volume: 134
• Pages of publication: 11035 - 11043
• a: 11.214 ± 0.002 Å
• b: 12.161 ± 0.002 Å
• c: 21.67 ± 0.004 Å
• α: 87.342 ± 0.003°
• β: 81.058 ± 0.003°
• γ: 65.693 ± 0.003°
• Cell volume: 2660 ± 0.8 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.075
• Residual factor for significantly intense reflections: 0.05
• Weighted residual factors for significantly intense reflections: 0.1114
• Weighted residual factors for all reflections included in the refinement: 0.1255
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No