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Information card for entry 4118872
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Coordinates | 4118872.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | Dimitry-180 |
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Formula | C52 H109 Li3 O4 Si5 |
Calculated formula | C52 H109 Li3 O4 Si5 |
Title of publication | Synthesis of Silenyllithiums Li(R'3Si)Si=C(SiR3)(1-Ad) via Transient Silyne-Silylidene Intermediates |
Authors of publication | Lieby Zborovsky; Roman Dobrovetsky; Mark Botoshansky; Dmitry Bravo-Zhivotovskii; Yitzhak Apeloig |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2012 |
Journal volume | 134 |
Pages of publication | 18229 - 18232 |
a | 21.474 ± 0.004 Å |
b | 11.565 ± 0.002 Å |
c | 50.33 ± 0.01 Å |
α | 90° |
β | 92.25 ± 0.01° |
γ | 90° |
Cell volume | 12490 ± 4 Å3 |
Cell temperature | 240 ± 1 K |
Ambient diffraction temperature | 240 ± 1 K |
Number of distinct elements | 5 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0908 |
Residual factor for significantly intense reflections | 0.0527 |
Weighted residual factors for significantly intense reflections | 0.1354 |
Weighted residual factors for all reflections included in the refinement | 0.144 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.919 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4118872.html
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Users of the data should acknowledge the original authors of the
structural data.