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Information card for entry 4119159
Preview
Coordinates | 4119159.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C34 H42 Cl2 F2 N4 O2 Rh2 |
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Calculated formula | C34 H42 Cl2 F2 N4 O2 Rh2 |
Title of publication | Rhodium(III)-Catalyzed N-Nitroso-Directed C-H Olefination of Arenes. High-Yield, Versatile Coupling under Mild Conditions |
Authors of publication | Baoqing Liu; Yang Fan; Yang Gao; Chao Sun; Cheng Xu; Jin Zhu |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2013 |
Journal volume | 135 |
Pages of publication | 468 - 473 |
a | 7.889 ± 0.005 Å |
b | 8.303 ± 0.005 Å |
c | 14.135 ± 0.008 Å |
α | 77.9 ± 0.007° |
β | 78.893 ± 0.007° |
γ | 68.444 ± 0.008° |
Cell volume | 835.2 ± 0.9 Å3 |
Cell temperature | 298 ± 2 K |
Ambient diffraction temperature | 298 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0511 |
Residual factor for significantly intense reflections | 0.0432 |
Weighted residual factors for significantly intense reflections | 0.1361 |
Weighted residual factors for all reflections included in the refinement | 0.1527 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.177 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4119159.html
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