Information card for entry 4119251

Structure parameters

• Formula: C14 H177 Co2.5 K10 N7 O205 Se3 W42.5
• Calculated formula: C3.8 Co2.5 K9.4 N5 O183.2 Se3 W42.5
• Title of publication: One-Pot versus Sequential Reactions in the Self-Assembly of Gigantic Nanoscale Polyoxotungstates
• Authors of publication: Jing Gao; Jun Yan; Sebastian Beeg; De-Liang Long; Leroy Cronin
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2013
• Journal volume: 135
• Pages of publication: 1796 - 1805
• a: 20.9947 ± 0.0004 Å
• b: 23.7936 ± 0.0004 Å
• c: 24.411 ± 0.0004 Å
• α: 104.343 ± 0.002°
• β: 107.505 ± 0.002°
• γ: 103.022 ± 0.002°
• Cell volume: 10657.3 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1226
• Residual factor for significantly intense reflections: 0.0472
• Weighted residual factors for significantly intense reflections: 0.0938
• Weighted residual factors for all reflections included in the refinement: 0.1065
• Goodness-of-fit parameter for all reflections included in the refinement: 0.811
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No