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Information card for entry 4119638
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Coordinates | 4119638.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | 4a |
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Formula | C26 H36 Cl4 N2 W |
Calculated formula | C26 H36 Cl4 N2 W |
SMILES | C1C=[N]([W]([N]=1c1c(cccc1C(C)C)C(C)C)(Cl)(Cl)(Cl)Cl)c1c(cccc1C(C)C)C(C)C |
Title of publication | Salt-Free Reducing Reagent of Bis(trimethylsilyl)cyclohexadiene Mediates Multielectron Reduction of Chloride Complexes of W(VI) and W(IV) |
Authors of publication | Hayato Tsurugi; Hiromasa Tanahashi; Haruka Nishiyama; Waldemar Fegler; Teruhiko Saito; Andreas Sauer; Jun Okuda; Kazushi Mashima |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2013 |
Journal volume | 135 |
Pages of publication | 5986 - 5989 |
a | 12.7024 ± 0.0017 Å |
b | 21.299 ± 0.003 Å |
c | 10.4913 ± 0.0015 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2838.4 ± 0.7 Å3 |
Cell temperature | 113 ± 2 K |
Ambient diffraction temperature | 113 ± 2 K |
Number of distinct elements | 5 |
Space group number | 62 |
Hermann-Mauguin space group symbol | P n m a |
Hall space group symbol | -P 2ac 2n |
Residual factor for all reflections | 0.1223 |
Residual factor for significantly intense reflections | 0.1107 |
Weighted residual factors for significantly intense reflections | 0.3289 |
Weighted residual factors for all reflections included in the refinement | 0.3509 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.552 |
Diffraction radiation wavelength | 0.71075 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4119638.html
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Users of the data should acknowledge the original authors of the
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