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Information card for entry 4119641
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Coordinates | 4119641.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | 7 |
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Formula | C68 H93 Cl5 N5 W2 |
Calculated formula | C68 H93 Cl5 N5 W2 |
Title of publication | Salt-Free Reducing Reagent of Bis(trimethylsilyl)cyclohexadiene Mediates Multielectron Reduction of Chloride Complexes of W(VI) and W(IV) |
Authors of publication | Hayato Tsurugi; Hiromasa Tanahashi; Haruka Nishiyama; Waldemar Fegler; Teruhiko Saito; Andreas Sauer; Jun Okuda; Kazushi Mashima |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2013 |
Journal volume | 135 |
Pages of publication | 5986 - 5989 |
a | 11.85 ± 0.004 Å |
b | 12.83 ± 0.004 Å |
c | 25.097 ± 0.008 Å |
α | 80.947 ± 0.01° |
β | 83.188 ± 0.009° |
γ | 74.034 ± 0.006° |
Cell volume | 3611 ± 2 Å3 |
Cell temperature | 113 ± 2 K |
Ambient diffraction temperature | 113 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0593 |
Residual factor for significantly intense reflections | 0.0465 |
Weighted residual factors for significantly intense reflections | 0.1138 |
Weighted residual factors for all reflections included in the refinement | 0.1239 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.063 |
Diffraction radiation wavelength | 0.71075 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4119641.html
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Users of the data should acknowledge the original authors of the
structural data.