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Information card for entry 4119701
Preview
Coordinates | 4119701.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C28 H58 Fe N2 P4 Si |
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Calculated formula | C28 H58 Fe N2 P4 Si |
SMILES | [Fe]12([Si]3([N](=C(N3C(C)(C)C)c3ccccc3)C(C)(C)C)C)([P](C)(CC[P]2(C)C)C)[P](C)(CC[P]1(C)C)C |
Title of publication | Electron-Rich N-Heterocyclic Silylene (NHSi)-Iron Complexes: Synthesis, Structures, and Catalytic Ability of an Isolable Hydridosilylene-Iron Complex |
Authors of publication | Burgert Blom; Stephan Enthaler; Shigeyoshi Inoue; Elisabeth Irran; Matthias Driess |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2013 |
Journal volume | 135 |
Pages of publication | 6703 - 6713 |
a | 36.85 ± 0.005 Å |
b | 9.3961 ± 0.0005 Å |
c | 23.976 ± 0.003 Å |
α | 90° |
β | 123.614 ± 0.016° |
γ | 90° |
Cell volume | 6913.5 ± 1.8 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 6 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.1278 |
Residual factor for significantly intense reflections | 0.1083 |
Weighted residual factors for significantly intense reflections | 0.2252 |
Weighted residual factors for all reflections included in the refinement | 0.2337 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.181 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4119701.html
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