Information card for entry 4119807

Structure parameters

• Formula: C44 H78 P2 Pd Si8 Sn
• Calculated formula: C44 H78 P2 Pd Si8 Sn
• SMILES: [Sn]1([Pd]2([P](CC[P]2(c2ccccc2)c2ccccc2)(c2ccccc2)c2ccccc2)[Si]1([Si](C)(C)C)[Si](C)(C)C)([Si](C)(C)C)[Si]([Si](C)(C)C)([Si](C)(C)C)[Si](C)(C)C
• Title of publication: Coordination Chemistry of Disilylated Stannylenes with Group 10 d10 Transition Metals: Silastannene vs Stannylene Complexation
• Authors of publication: Henning Arp; Christoph Marschner; Judith Baumgartner; Patrick Zark; Thomas Müller
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2013
• Journal volume: 135
• Pages of publication: 7949 - 7959
• a: 13.201 ± 0.003 Å
• b: 21.731 ± 0.004 Å
• c: 19.717 ± 0.004 Å
• α: 90°
• β: 97.37 ± 0.03°
• γ: 90°
• Cell volume: 5610 ± 2 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0539
• Residual factor for significantly intense reflections: 0.0493
• Weighted residual factors for significantly intense reflections: 0.1013
• Weighted residual factors for all reflections included in the refinement: 0.1033
• Goodness-of-fit parameter for all reflections included in the refinement: 1.253
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No