Crystallography Open Database

Information card for entry 4119836

4119835 << 4119836 >> 4119837

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Coordinates	4119836.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C86 H92 Cu2 F12 N8 O26 Rh4 S4
Calculated formula	C84 H84 Cu2 F6 N8 O20 Rh4 S2
Title of publication	Cp*Rh-Based Heterometallic Metallarectangles: Size-Dependent Borromean Link Structures and Catalytic Acyl Transfer
Authors of publication	Sheng-Li Huang; Yue-Jian Lin; T. S. Andy Hor; Guo-Xin Jin
Journal of publication	Journal of the American Chemical Society
Year of publication	2013
Journal volume	135
Pages of publication	8125 - 8128
a	18.1252 ± 0.0018 Å
b	17.8848 ± 0.0018 Å
c	18.1859 ± 0.0019 Å
α	90°
β	115.66 ± 0.002°
γ	90°
Cell volume	5313.9 ± 0.9 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	8
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1266
Residual factor for significantly intense reflections	0.1096
Weighted residual factors for significantly intense reflections	0.3247
Weighted residual factors for all reflections included in the refinement	0.3505
Goodness-of-fit parameter for all reflections included in the refinement	1.461
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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