Information card for entry 4119912

Structure parameters

• Formula: C254 H317 Cd18 Cl8 Gd6 N18 O92
• Calculated formula: C254 H317 Cd18 Cl8 Gd6 N18 O92
• Title of publication: Anion-Dependent Self-Assembly of Near-Infrared Luminescent 24- and 32-Metal Cd-Ln Complexes with Drum-like Architectures
• Authors of publication: Xiaoping Yang; Desmond Schipper; Richard A. Jones; Lauren A. Lytwak; Bradley J. Holliday; Shaoming Huang
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2013
• Journal volume: 135
• Pages of publication: 8468 - 8471
• a: 51.282 ± 0.007 Å
• b: 51.282 ± 0.007 Å
• c: 24.391 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 55551 ± 16 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 1 K
• Number of distinct elements: 7
• Space group number: 147
• Hermann-Mauguin space group symbol: P -3
• Hall space group symbol: -P 3
• Residual factor for all reflections: 0.1026
• Residual factor for significantly intense reflections: 0.0674
• Weighted residual factors for significantly intense reflections: 0.1765
• Weighted residual factors for all reflections included in the refinement: 0.1926
• Goodness-of-fit parameter for all reflections included in the refinement: 1.102
• Diffraction radiation wavelength: 0.710747 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No