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Information card for entry 4120023
Preview
Coordinates | 4120023.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C62 H115 K2 O13.5 Si4 Tb |
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Calculated formula | C62 H115 K2 O13.5 Si4 Tb |
Title of publication | Completing the Series of +2 Ions for the Lanthanide Elements: Synthesis of Molecular Complexes of Pr2+, Gd2+, Tb2+, and Lu2+ |
Authors of publication | Matthew R. MacDonald; Jefferson E. Bates; Joseph W. Ziller; Filipp Furche; William J. Evans |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2013 |
Journal volume | 135 |
Pages of publication | 9857 - 9868 |
a | 25.7503 ± 0.0014 Å |
b | 11.6143 ± 0.0006 Å |
c | 26.3215 ± 0.0014 Å |
α | 90° |
β | 104.005 ± 0.0006° |
γ | 90° |
Cell volume | 7638 ± 0.7 Å3 |
Cell temperature | 143 ± 2 K |
Ambient diffraction temperature | 143 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0299 |
Residual factor for significantly intense reflections | 0.0254 |
Weighted residual factors for significantly intense reflections | 0.0669 |
Weighted residual factors for all reflections included in the refinement | 0.0695 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.035 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4120023.html
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