Information card for entry 4120091

Structure parameters

• Formula: C36 H36 Si
• Calculated formula: C36 H36 Si
• Title of publication: Dibenzosilanorbornadienyl Cations and Their Fragmentation into Silyliumylidenes
• Authors of publication: Claudia Gerdes; Wolfgang Saak; Detlev Haase; Thomas Müller
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2013
• Journal volume: 135
• Pages of publication: 10353 - 10361
• a: 12.4831 ± 0.0004 Å
• b: 16.0535 ± 0.0006 Å
• c: 14.5104 ± 0.0005 Å
• α: 90°
• β: 96.848 ± 0.002°
• γ: 90°
• Cell volume: 2887.1 ± 0.17 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 3
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0996
• Residual factor for significantly intense reflections: 0.0628
• Weighted residual factors for significantly intense reflections: 0.1558
• Weighted residual factors for all reflections included in the refinement: 0.1765
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No