Crystallography Open Database

Information card for entry 4120279

4120278 << 4120279 >> 4120280

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Coordinates	4120279.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C58 H118 N2 O16 Si4 U
Calculated formula	C58 H118 N2 O16 Si4 U
Title of publication	Tuning Uranium-Nitrogen Multiple Bond Formation with Ancillary Siloxide Ligands
Authors of publication	Clément Camp; Jacques Pécaut; Marinella Mazzanti
Journal of publication	Journal of the American Chemical Society
Year of publication	2013
Journal volume	135
Pages of publication	12101 - 12111
a	24.5649 ± 0.0008 Å
b	13.263 ± 0.0003 Å
c	25.9619 ± 0.0008 Å
α	90°
β	118.606 ± 0.004°
γ	90°
Cell volume	7426 ± 0.5 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0274
Residual factor for significantly intense reflections	0.0234
Weighted residual factors for significantly intense reflections	0.0529
Weighted residual factors for all reflections included in the refinement	0.0542
Goodness-of-fit parameter for all reflections included in the refinement	1.049
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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