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Information card for entry 4120355
Preview
Coordinates | 4120355.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C47.5 H36 B Cl F15 N2 O2 Rh |
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Calculated formula | C47.5 H36 B Cl F15 N2 O2 Rh |
Title of publication | Iridium(I) Complexes with Anionic N-Heterocyclic Carbene Ligands as Catalysts for the Hydrogenation of Alkenes in Nonpolar Media |
Authors of publication | Eugene L. Kolychev; Sabrina Kronig; Kai Brandhorst; Matthias Freytag; Peter G. Jones; Matthias Tamm |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2013 |
Journal volume | 135 |
Pages of publication | 12448 - 12459 |
a | 11.7736 ± 0.0004 Å |
b | 11.9723 ± 0.0004 Å |
c | 17.8593 ± 0.0006 Å |
α | 73.048 ± 0.004° |
β | 77.719 ± 0.004° |
γ | 70.396 ± 0.004° |
Cell volume | 2249.92 ± 0.15 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0349 |
Residual factor for significantly intense reflections | 0.0276 |
Weighted residual factors for significantly intense reflections | 0.0587 |
Weighted residual factors for all reflections included in the refinement | 0.0617 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.041 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4120355.html
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