Crystallography Open Database

Information card for entry 4120477

4120476 << 4120477 >> 4120478

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Coordinates	4120477.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C15 H25 F3 N2 Sn
Calculated formula	C15 H25 F3 N2 Sn0.996
Title of publication	Synthetic Access to a Hydrocarbon-Soluble Trifluorinated Ge(II) Compound and its Sn(II) Congener.
Authors of publication	Samuel, Prinson P.; Li, Yan; Roesky, Herbert W.; Chevelkov, Veniamin; Lange, Adam; Burkhardt, Anja; Dittrich, Birger
Journal of publication	Journal of the American Chemical Society
Year of publication	2014
Journal volume	136
Journal issue	4
Pages of publication	1292 - 1295
a	9.573 ± 0.005 Å
b	17.473 ± 0.004 Å
c	11.177 ± 0.012 Å
α	90°
β	105.99 ± 0.05°
γ	90°
Cell volume	1797 ± 2 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0377
Residual factor for significantly intense reflections	0.0362
Weighted residual factors for significantly intense reflections	0.098
Weighted residual factors for all reflections included in the refinement	0.0993
Goodness-of-fit parameter for all reflections included in the refinement	1.072
Diffraction radiation wavelength	0.6199 Å
Diffraction radiation type	synchrotron
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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