Information card for entry 4120590

Structure parameters

• Formula: C12 H16 Cu4 N4 O8
• Calculated formula: C12 H16 Cu4 N4 O8
• Title of publication: Photoinduced, copper-catalyzed alkylation of amides with unactivated secondary alkyl halides at room temperature.
• Authors of publication: Do, Hien-Quang; Bachman, Shoshana; Bissember, Alex C.; Peters, Jonas C.; Fu, Gregory C.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2014
• Journal volume: 136
• Journal issue: 5
• Pages of publication: 2162 - 2167
• a: 12.2871 ± 0.0002 Å
• b: 12.2871 ± 0.0002 Å
• c: 46.554 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7028.4 ± 0.2 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 122
• Hermann-Mauguin space group symbol: I -4 2 d
• Hall space group symbol: I -4 2bw
• Residual factor for all reflections: 0.0464
• Residual factor for significantly intense reflections: 0.0332
• Weighted residual factors for significantly intense reflections: 0.0636
• Weighted residual factors for all reflections included in the refinement: 0.0677
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No