Information card for entry 4120677

Structure parameters

• Formula: C40 H33 B2 F15 Si2
• Calculated formula: C40 H33 B2 F15 Si2
• Title of publication: Borole formation by 1,1-carboboration.
• Authors of publication: Ge, Fang; Kehr, Gerald; Daniliuc, Constantin G.; Erker, Gerhard
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2014
• Journal volume: 136
• Journal issue: 1
• Pages of publication: 68 - 71
• a: 11.6645 ± 0.0004 Å
• b: 12.2645 ± 0.0005 Å
• c: 18.5329 ± 0.0007 Å
• α: 108.563 ± 0.002°
• β: 96.887 ± 0.002°
• γ: 98.819 ± 0.002°
• Cell volume: 2443.04 ± 0.16 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0601
• Residual factor for significantly intense reflections: 0.0494
• Weighted residual factors for significantly intense reflections: 0.1409
• Weighted residual factors for all reflections included in the refinement: 0.1489
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No