Information card for entry 4120698

Structure parameters

• Formula: C38 H95 K N5 O6.5 S Si6 U
• Calculated formula: C38 H54 K N5 O6.5 S Si6 U
• Title of publication: Synthesis of uranium-ligand multiple bonds by cleavage of a trityl protecting group.
• Authors of publication: Smiles, Danil E.; Wu, Guang; Hayton, Trevor W.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2014
• Journal volume: 136
• Journal issue: 1
• Pages of publication: 96 - 99
• a: 11.2243 ± 0.0003 Å
• b: 16.4779 ± 0.0004 Å
• c: 32.1639 ± 0.0008 Å
• α: 90°
• β: 91.774 ± 0.002°
• γ: 90°
• Cell volume: 5946 ± 0.3 ų
• Cell temperature: 104 ± 2 K
• Ambient diffraction temperature: 104 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0692
• Residual factor for significantly intense reflections: 0.0512
• Weighted residual factors for significantly intense reflections: 0.1473
• Weighted residual factors for all reflections included in the refinement: 0.1593
• Goodness-of-fit parameter for all reflections included in the refinement: 1.148
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No