Information card for entry 4120719

Structure parameters

• Common name: NiL
• Formula: C42.5 H67 N4 Ni P3
• Calculated formula: C42.5 H67 N4 Ni P3
• Title of publication: Systematic Variation of Metal-Metal Bond Order in Metal-Chromium Complexes
• Authors of publication: Laura J. Clouston; Randall B. Siedschlag; P. Alex Rudd; Nora Planas; Shuxian Hu; Adam D. Miller; Laura Gagliardi; Connie C. Lu
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2013
• Journal volume: 135
• Pages of publication: 13142 - 13148
• a: 11.373 ± 0.001 Å
• b: 14.0502 ± 0.0011 Å
• c: 14.1811 ± 0.001 Å
• α: 71.846 ± 0.001°
• β: 80.484 ± 0.001°
• γ: 82.265 ± 0.001°
• Cell volume: 2115.3 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0636
• Residual factor for significantly intense reflections: 0.045
• Weighted residual factors for significantly intense reflections: 0.112
• Weighted residual factors for all reflections included in the refinement: 0.1239
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No