Crystallography Open Database

Information card for entry 4120788

4120787 << 4120788 >> 4120789

Preview

Coordinates	4120788.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H40 P2 Sn2
Calculated formula	C40 H40 P2 Sn2
Title of publication	Activation of a σ-SnSn Bond at Copper, Followed by Double Addition to an Alkyne
Authors of publication	Nicolas Lassauque; Pauline Gualco; Sonia Mallet-Ladeira; Karinne Miqueu; Abderrahmane Amgoune; Didier Bourissou
Journal of publication	Journal of the American Chemical Society
Year of publication	2013
Journal volume	135
Pages of publication	13827 - 13834
a	20.0617 ± 0.0013 Å
b	8.662 ± 0.0006 Å
c	21.4146 ± 0.0014 Å
α	90°
β	90.5 ± 0.003°
γ	90°
Cell volume	3721.2 ± 0.4 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0413
Residual factor for significantly intense reflections	0.0276
Weighted residual factors for significantly intense reflections	0.0855
Weighted residual factors for all reflections included in the refinement	0.1104
Goodness-of-fit parameter for all reflections included in the refinement	1.204
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4120788.html