Information card for entry 4120928

Structure parameters

• Formula: C34.5 H52 Au Cl3 F6 N5 Sb
• Calculated formula: C34.5 H52 Au Cl3 F6 N5 Sb
• Title of publication: Gold-Mediated Expulsion of Dinitrogen from Organic Azides
• Authors of publication: Chandrakanta Dash; Muhammed Yousufuddin; Thomas R. Cundari; H. V. Rasika Dias
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2013
• Journal volume: 135
• Pages of publication: 15479 - 15488
• a: 16.861 ± 0.002 Å
• b: 12.0404 ± 0.0014 Å
• c: 21.422 ± 0.003 Å
• α: 90°
• β: 105.626 ± 0.002°
• γ: 90°
• Cell volume: 4188.2 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100.15 K
• Number of distinct elements: 7
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0607
• Residual factor for significantly intense reflections: 0.0545
• Weighted residual factors for significantly intense reflections: 0.1333
• Weighted residual factors for all reflections included in the refinement: 0.1381
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes