Crystallography Open Database

Information card for entry 4120930

4120929 << 4120930 >> 4120931

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Structure parameters

Formula	C34 H51 Au Cl2 F6 N3 Sb
Calculated formula	C34 H51 Au Cl2 F6 N3 Sb
Title of publication	Gold-Mediated Expulsion of Dinitrogen from Organic Azides
Authors of publication	Chandrakanta Dash; Muhammed Yousufuddin; Thomas R. Cundari; H. V. Rasika Dias
Journal of publication	Journal of the American Chemical Society
Year of publication	2013
Journal volume	135
Pages of publication	15479 - 15488
a	22.316 ± 0.002 Å
b	11.1178 ± 0.0011 Å
c	18.4682 ± 0.0018 Å
α	90°
β	121.874 ± 0.001°
γ	90°
Cell volume	3891.1 ± 0.6 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0398
Residual factor for significantly intense reflections	0.0363
Weighted residual factors for significantly intense reflections	0.087
Weighted residual factors for all reflections included in the refinement	0.0891
Goodness-of-fit parameter for all reflections included in the refinement	1.013
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	Yes

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